Column:BeksichStPolyamine,5um(53x4.6mm)流动相:A=20mMTRIS-pH7B=1MNH4OAc-pH7梯度:0-100%Bin20min.监测波长:280nm,流速:1ml/minLactoglobuline:乳球蛋白BSA:牛血清白蛋白cytochrome细胞色素

Column:BeksichGTurbo100ODS,1.5um(33x4.6mm)流动相:ACN/0,1%TFA(35/65),流速:1.5ml/min.Benzodiazepine苯二氮1=Clonazepam氯*/氯硝安定2=Diazepam安定

Columns:150x4.6mmEluent:MeCN/50mMKH2PO450/50,pH3,Flowrate:1ml/min1:primidone:普里米酮；去氧；扑痫酮2:Phenobarbitone:3:carbamazepine卡马西平,立痛定；卡巴咪嗪；酰胺咪嗪；氨甲酰氮草

BeksichSt120BS-C23,(100x4.6mm)流动相:A=0.1%TFA,B=0,1%TFAinACN梯度:15-40%Bin10min.,流速:1ml/min监测波长：230nm

同时分析1-ａnd2-val.阳离子Column:BeksichCat,5um(or7um)(125x4.6mm)Eluent:5.0mM柠檬酸+0.5mM2,6吡啶二甲酸or0.6mM抗坏血酸+3.3mM磷酸pH2,7

AnioneswithSuppressorColumn:BeksichGelAXS(150x4mm)Eluent:1.7mM碳酸氢钠/1.8mM碳酸钠/0.1mM硫氰酸钠温度:RT流速:2ml/min.进样量:100ulF：氟离子，Cl：氯离子，Nitrite：亚硝酸盐，Bromide：溴化物，nitrate；硝酸，Phosphate：磷酸盐，Sulfate：硫酸Column:BeksichGelAX,10um(150x4mm)Eluent:mM邻苯二甲酸氢钾(pH6.0)流...

Beksich-TG-Chiral,5um(250x3mm),梯度:50mM醋酸缓冲液pH4,5/乙腈(1/1),流速:0,6ml/min检测器:UV254nm1=D+L-Serin/D+L-丝氨酸2=D+L-缬氨酸3=D+L-色氨酸